Synthesis of nano-CeO<sub>2</sub> powder by detonation method

Han Zhi-wei; Xie Li-feng; Deng Ji-ping; Xie Yi-chao; Chen Ji-yang

doi:10.11883/1001-1455(2014)01-0106-05

Volume 34 Issue 1

Mar. 2014

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Han Zhi-wei, Xie Li-feng, Deng Ji-ping, Xie Yi-chao, Chen Ji-yang. Synthesis of nano-CeO2 powder by detonation method[J]. Explosion And Shock Waves, 2014, 34(1): 106-110. doi: 10.11883/1001-1455(2014)01-0106-05

Citation:

Han Zhi-wei, Xie Li-feng, Deng Ji-ping, Xie Yi-chao, Chen Ji-yang. Synthesis of nano-CeO₂ powder by detonation method[J]. Explosion And Shock Waves, 2014, 34(1): 106-110. doi: 10.11883/1001-1455(2014)01-0106-05

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Synthesis of nano-CeO₂ powder by detonation method

doi: 10.11883/1001-1455(2014)01-0106-05

School of Chemical Engineering, Nanjing University of Science and Technology, Nanjing 210094, Jiangsu, China

Funds: Supported by the National Natural Science Foundation of China (11102091)

Received Date: 2012-08-28
Rev Recd Date: 2012-12-14
Publish Date: 2014-01-25

Abstract

Abstract

The blasting agentwas prepared by choosing Ce(NO₃)₃·6H₂O as themajor ingredient to synthesize nano-CeO₂ powder by the detonation method.The as-synthesized productswere characterized by X-ray diffraction(XRD)and transmission electron microscopy(TEM).Thereby, the influences of the initiation manners on the crystallization, particle size andmorphology of the as-synthesized productswere analyzed.The results indicate that CeO₂spherical nano-particleswhose crystal structure belongs to cubic system can be synthesized by using the blasting agent in which Ce(NO₃)₃·6H₂O acting as themajor ingredient.And it is an effectivemethod to decrease the particle size and improve the spherification of nano-CeO₂ by increasing the detonation velocity of the blasting agent.
- mechanics of explosion,
- nano-CeO₂ powder,
- detonation synthesis,
- blasting agent,
- cubic system,
- Ce(NO₃)₃·6H₂O,
- XRD,
- TEM

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References(19)

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