Shocksynthesisandcharacterizationofcarbonnitride

YU Yan-wu; LIU Yu-cun; ZHENGXin; ZHANG Hai-long

doi:10.11883/1001-1455(2011)02-0113-06

Volume 31 Issue 2

May 2014

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YU Yan-wu, LIU Yu-cun, ZHENGXin, ZHANG Hai-long. Shocksynthesisandcharacterizationofcarbonnitride[J]. Explosion And Shock Waves, 2011, 31(2): 113-118. doi: 10.11883/1001-1455(2011)02-0113-06

Citation:

YU Yan-wu, LIU Yu-cun, ZHENGXin, ZHANG Hai-long. Shocksynthesisandcharacterizationofcarbonnitride[J]. Explosion And Shock Waves, 2011, 31(2): 113-118. doi: 10.11883/1001-1455(2011)02-0113-06

YU Yan-wu, LIU Yu-cun, ZHENGXin, ZHANG Hai-long. Shocksynthesisandcharacterizationofcarbonnitride[J]. Explosion And Shock Waves, 2011, 31(2): 113-118. doi: 10.11883/1001-1455(2011)02-0113-06

Citation:

YU Yan-wu, LIU Yu-cun, ZHENGXin, ZHANG Hai-long. Shocksynthesisandcharacterizationofcarbonnitride[J]. Explosion And Shock Waves, 2011, 31(2): 113-118. doi: 10.11883/1001-1455(2011)02-0113-06

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Shocksynthesisandcharacterizationofcarbonnitride

doi: 10.11883/1001-1455(2011)02-0113-06

1.
SchoolofChemicalEngineeringandEnvironment,NorthUniversityofChina,
2.
Taiyuan 030051,Shanxi,China;

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Corresponding author: YU Yan-wu
Publish Date: 2011-03-25

Abstract

Abstract

Carbonnitridepowderswith C N bondswerepreparedbytaking1,3,5-trinitro-1,3,5- triazacyclohexane(RDX)asthehigh-temperature,high-pressuresourceaswellasdicyandiamide (C2H4N4)astheprimaryprecursor.Themorphology,compositionandstructureoftheproducts werecharacterizedbyusingscanningelectronmicroscopy(SEM),X-raydiffraction(XRD),Fourier transforminfrared(FTIR)andX-rayphotoelectronspectroscopy(EDS).Theresultsshowthatall the C?N bondsandthegreatmassofthe CN bondsintheprecursoraredestroyedandturned intoC3N4crystalmainlywith C N bonds.XRDresultssuggestthattheproductincludes-C3N4, -C3N4andgraphite-C3N4crystals.Somehexagonalparticlesof2minsizeareobservedinthescanningelectronmicroscopy. Nitrogencontentintheproductscanbeeffectivelyimprovedbyadding5- aminotetrazole(CH3N5)inprecursors.
- mechanicsofexplosion,
- carbonnitride,
- shocksynthesis,
- dicyandiamide,
- RDX